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AAS

Metal element quantitation
🎯 Difficulty ★★★ Advanced Duration About 3–5 h 🎯 Use Trace determination of metals such as Pb, Cd, As, Hg and Cu
📖 Principle
Ground-state atoms absorb characteristic wavelengths or excited atoms emit; intensity is proportional to concentration
Below are 5 steps. Open each to see how to do it and add products to your shared list.

📋 Workflow

Full workflow, products add-to-cart directly
1

Sample digestion

60 min
Digest the sample by microwave or wet digestion into a clear solution
💡 Tip HNO₃–H₂O₂ system is common
⚠️ Caution Work in fume hood to avoid acid fumes
🧪 Materials for this step (click to shop by spec/brand)
2

Calibration curve

30 min
Dilute metal stock standards into a calibration series
💡 Tip Add matrix modifier to reduce interference
⚠️ Caution Match standard matrix with the sample
🧪 Materials for this step (click to shop by spec/brand)
3

Instrument setup & ignition

30 min
Install hollow cathode lamp; tune flame or graphite furnace parameters and ignite
💡 Tip Flame suits mg/L; graphite furnace suits μg/L
⚠️ Caution Ventilate to avoid flashback risk
🧪 Materials for this step (click to shop by spec/brand)
4

Sample measurement

40 min
Measure absorbance of blank, standards and samples in sequence
💡 Tip Subtract blank for each batch
⚠️ Caution Dilute high samples within linear range
🧪 Materials for this step (click to shop by spec/brand)
5

Quant & report

30 min
Calculate sample metal concentration from the calibration curve with QC
💡 Tip Use spike recovery to assess accuracy
⚠️ Caution Keep units consistent with dilution factor
🧪 Materials for this step (click to shop by spec/brand)

⚠️ 5 Common Beginner Mistakes

  • Incomplete digestion causing low results
  • Unremoved matrix interference
  • Improper flame parameters lowering sensitivity
  • Blank contamination raising background
  • Standard matrix mismatching the sample

❓ FAQ

+AAS or ICP-MS?
Use AAS for routine; ICP-MS for multi-element trace.
+Notes for mercury?
Use cold vapor/hydride generation to avoid volatility loss.
+Dilute samples?
Dilute to fall within the linear range.

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Data authenticity: Product categories from JW Supply Chain standard taxonomy; method→step→product connected. Last updated: 2026-08-23 · v3.0